{"id":9,"date":"2015-12-18T09:20:17","date_gmt":"2015-12-18T00:20:17","guid":{"rendered":"https:\/\/www2.tagen.tohoku.ac.jp\/lab\/caf\/?page_id=9"},"modified":"2024-09-25T14:11:08","modified_gmt":"2024-09-25T05:11:08","slug":"molecular-structure","status":"publish","type":"page","link":"https:\/\/www2.tagen.tohoku.ac.jp\/lab\/caf\/molecular-structure\/","title":{"rendered":"\u5206\u5b50\u69cb\u9020\u89e3\u6790\u88c5\u7f6e"},"content":{"rendered":"

\u6838\u78c1\u6c17\u5171\u9cf4\u88c5\u7f6e (\u6eb6\u6db2\u7528NMR 400\/500\/600MHz)<\/h2>\n

\u6a5f\u5668\u540d\uff1a\u6838\u78c1\u6c17\u5171\u9cf4\u88c5\u7f6e NMR 400\/500\/600 MHz
\n\u88fd\u9020\u5143\uff1aBruker
\n\u578b\u756a\u3000\uff1aAVANCEIII400\u578b, AVANCEIII500\u578b, AVANCEIII600\u578b
\n\u751f\u7406\u6d3b\u6027\u5929\u7136\u7269\u304b\u3089\u4f4e\u5206\u5b50\u6709\u6a5f\u5316\u5408\u7269\u307e\u3067\u591a\u7a2e\u591a\u69d8\u306a\u5316\u5408\u7269\u306e\u69cb\u9020\u540c \u5b9a\u306b\u4f7f\u7528\u53ef\u80fd\u3002
\n500 MHz:\u591a\u6838\u30d7\u30ed\u30fc\u30d6\u3092\u5099\u3048\u3001\u6e29\u5ea6\u53ef\u5909\u3082\u53ef\u80fd\u3002 (1<\/sup>H, 19<\/sup>F, 31<\/sup>P\u301c109<\/sup>Ag \/ \u2212150\u301c+180 \u00b0C)
\n600 MHz:Cryoprobe\u3092\u642d\u8f09\u300219F\u6e2c\u5b9a\u306b\u3082\u5bfe\u5fdc\u53ef\u80fd\u3002
\n\u6240\u5185\u30fb\u6240\u5916\u306e\u591a\u6570\u306e\u7814\u7a76\u5ba4\u3067\u4f7f\u7528\u5b9f\u7e3e\u304c\u3042\u308b\u3002<\/p>\n

\"\u5206\u5b50\u69cb\u9020\u89e3\u6790\u88c5\u7f6e21\u6838\u78c1\u6c17\u5171\u9cf4\u88c5\u7f6e<\/a>\u00a0\"\u5206\u5b50\u69cb\u9020\u89e3\u6790\u88c5\u7f6e21\u6838\u78c1\u6c17\u5171\u9cf4\u88c5\u7f6e<\/a>\u00a0\"\u5206\u5b50\u69cb\u9020\u89e3\u6790\u88c5\u7f6e21\u6838\u78c1\u6c17\u5171\u9cf4\u88c5\u7f6e<\/a><\/p>\n

\u8a2d\u7f6e\u5834\u6240\uff1a
\n400 MHz:\u591a\u5143\u7269\u8cea\u79d1\u5b66\u7814\u7a76\u6240\u67712\u53f7\u99282109\u53f7\u5ba4(\u6eb6\u6db2\u7528NMR\u5ba4)
\n500 MHz:\u591a\u5143\u7269\u8cea\u79d1\u5b66\u7814\u7a76\u6240\u67712\u53f7\u99282109\u53f7\u5ba4(\u6eb6\u6db2\u7528NMR\u5ba4)
\n600 MHz:\u591a\u5143\u7269\u8cea\u79d1\u5b66\u7814\u7a76\u6240\u6771\u65e7\u9928126\u53f7\u5ba4(\u8d85\u4f1d\u5c0eNMR\u5ba4)
\n\u7ba1\u7406\u8005\uff1a\u548c\u7530\u5065\u5f66 \u6559\u6388
\n\u9023\u7d61\u5148\uff1a022-217-5608<\/div>\n

\u30ca\u30ce\u30c7\u30d0\u30a4\u30b9\u30a4\u30aa\u30f3\u30c0\u30a4\u30ca\u30df\u30af\u30b9\u8a08\u6e2c\u88c5\u7f6e(\u56fa\u4f53\u7528NMR)<\/h2>\n

\u6a5f\u5668\u540d\uff1aNMR\u30de\u30a4\u30af\u30ed\u30a4\u30e1\u30fc\u30b8\u30f3\u30b0\u30fb\u62e1\u6563\u4fc2\u6570\u6e2c\u5b9a\u88c5\u7f6e
\n\u88fd\u9020\u5143\uff1aBruker Biospin
\n\u578b\u756a\u3000\uff1aAvance 400
\n\uff13\u8ef8\u306e\u78c1\u5834\u52fe\u914d\u88c5\u7f6e\u3092\u88c5\u5099\u3057\u305f\u3001NMR\u30de\u30a4\u30af\u30ed\u30a4\u30e1\u30fc\u30b8\u30f3\u30b0\u30fb\u62e1\u6563\u4fc2\u6570\u6e2c\u5b9a\u7528\u3002 \u56fa\u4f53\u30b9\u30bf\u30c6\u30a3\u30c3\u30af\u306e\u30b9\u30da\u30af\u30c8\u30eb\u3001\u7de9\u548c\u6642\u9593\u306a\u3069\u3082\u6e2c\u5b9a\u53ef\u80fd\u3002
\n\u30bb\u30c3\u30c6\u30a3\u30f3\u30b0\u306b\u719f\u7df4\u3092\u8981\u3059\u308b\u305f\u3081\u3001\u5229\u7528\u306b\u3042\u305f\u3063\u3066\u306f\u4e8b\u524d\u306b\u62c5\u5f53\u8005\u3068\u5145\u5206\u306b\u76f8\u8ac7\u3059\u308b\u3053\u3068\u3002<\/p>\n

\"E11-1\"<\/a><\/p>\n

\u6a5f\u5668\u540d\uff1a\u56fa\u4f53\u9ad8\u5206\u89e3\u80fd\u6838\u78c1\u6c17\u5171\u9cf4\u88c5\u7f6e
\n\u88fd\u9020\u5143\uff1aBruker Biospin
\n\u578b\u756a\u3000\uff1aAvance 600
\n\u56fa\u4f53\u591a\u6838MAS\u5c02\u7528\u3002\u30d7\u30ed\u30fc\u30d6\u306f\u30011H\/19F\u300115N\u301c31P\u306e\u6e2c\u5b9a\u304c\u53ef\u80fd\u306a\u6c4e\u7528\u30d7\u30ed\u30fc\u30d6(\u30ed\u30fc\u30bf\u5f844mm (\u6700\u5927\u56de\u8ee2\u657025kHz)\u3068\u3001\u9ad8\u901fMAS \u7528\u306e\u30ed\u30fc\u30bf\u5f842.5mm(\u6700\u5927\u56de\u8ee2\u657035kHz))\u3068\u3001\u30ed\u30fc\u30bf\u5f844mm\u306eLow\u03b3(\u301c109Ag)\u7528\u30d7\u30ed\u30fc\u30d6\u304c\u4f7f\u7528\u53ef\u80fd\u3002
\n\u30d7\u30ed\u30fc\u30d6\u4ea4\u63db\u306f\u62c5\u5f53\u8005\u306e\u307f\u53ef\u80fd\u3002\u64cd\u4f5c\u306b\u3042\u305f\u3063\u3066\u306f\u6280\u8853\u8077\u54e1\u304c\u884c\u3046\u3002<\/p>\n

\"E11-3\"<\/a><\/p>\n

\u8a2d\u7f6e\u5834\u6240\uff1a\u30ca\u30ce\u30c6\u30af\u30cb\u30ab\u30eb\u30e9\u30dc (\u591a\u5143\u7269\u8cea\u79d1\u5b66\u7814\u7a76\u6240\u67713\u53f7\u9928128\u53f7\u5ba4\uff09
\n\u7ba1\u7406\u8005\uff1a\u5c0f\u4fe3\u5b5d\u4e45 \u6559\u6388
\n\u9023\u7d61\u5148:022\u2010217\u20105660(\u62c5\u5f53\u8005:\u6280\u8853\u8077\u54e1\u30fb\u5343\u8449)<\/div>\n


\n<\/p>\n

\u30d1\u30eb\u30b9EPR<\/h2>\n

\u6a5f\u5668\u540d\uff1a\u30d1\u30eb\u30b9EPR
\n\u88fd\u9020\u5143\uff1aBruker
\n\u578b\u756a\u3000\uff1aE580
\nBruker E580 CW\/pulse EPR\u88c5\u7f6e\u306f\u901a\u5e38\u306eCW EPR\u306b\u52a0\u3048\u3066pulse EPR, CW ENDOR,pulse ENDOR\u306e\u6e2c\u5b9a\u304c\u53ef\u80fd\u3002
\n4.3 K\u304b\u3089\u6e2c\u5b9a\u53ef\u80fd\u306a\u6975\u4f4e\u6e29\u30ec\u30be\u30cd\u30fc\u30bf\u3092\u4f7f\u7528\u3059\u308b\u5834\u5408\u306f\u3001\u4e8b\u524d\u306b\u62c5\u5f53\u8005\u3068\u76f8\u8ac7\u3059\u308b\u3053\u3068\u3002<\/p>\n

\"Jpeg\"<\/a><\/p>\n

\u8a2d\u7f6e\u5834\u6240\uff1a\u30ca\u30ce\u30c6\u30af\u30cb\u30ab\u30eb\u30e9\u30dc(\u591a\u5143\u7269\u8cea\u79d1\u5b66\u7814\u7a76\u6240\u67713\u53f7\u9928127\u53f7\u5ba4)
\n\u7ba1\u7406\u8005\uff1a \u8352\u6728\u4fdd\u5e78 \u51c6\u6559\u6388
\n\u9023\u7d61\u5148\uff1a 022\u2010217\u20105660(\u62c5\u5f53\u8005:\u6280\u8853\u8077\u54e1\u30fb\u5343\u8449)<\/div>\n

\u9ad8\u6e29NMR\u89e3\u6790\u88c5\u7f6e<\/h2>\n

\u6a5f\u5668\u540d\uff1a\u9ad8\u6e29NMR\u89e3\u6790\u88c5\u7f6e
\n\u88fd\u9020\u5143\uff1aJEOL RESONANCE
\n\u578b\u756a\u3000\uff1aJNM-ECA300WB FTNMR
\n\uff11H\/19F\u300115N\uff5e\uff13\uff11P\u306e\u6838\u7a2e\u306b\u5bfe\u5fdc\u3057\u305f\u56fa\u4f53\u7528NMR\u3002
\n\u30d7\u30ed\u30fc\u30d6\u306f25\u2103\uff5e500\u2103\u307e\u3067\u306e\u6e29\u5ea6\u7bc4\u56f2\u306b\u5bfe\u5fdc\u3057\u305f\u62e1\u6563\u30d7\u30ed\u30fc\u30d6\u3068\u3001\u30ed\u30fc\u30bf\u5f844\u339c(\u8a66\u6599\u56de\u8ee2\u657010\uff4bHz)\u306e\u56fa\u4f53MAS\u30d7\u30ed\u30fc\u30d6\u304c\u4f7f\u7528\u53ef\u80fd\u3002
\n\u30d7\u30ed\u30fc\u30d6\u4ea4\u63db\u306f\u62c5\u5f53\u8005\u306e\u307f\u53ef\u80fd\u3002\u64cd\u4f5c\u306b\u3042\u305f\u3063\u3066\u306f\u57fa\u672c\u7684\u306b\u62c5\u5f53\u8005\u304c\u884c\u3046\u3002<\/p>\n

\"\"<\/a><\/p>\n

\u8a2d\u7f6e\u5834\u6240\uff1a\u5171\u540c\u7814\u7a76\u68df K101
\n\u7ba1\u7406\u8005\uff1a \u5c0f\u4fe3\u5b5d\u4e45 \u6559\u6388
\n\u9023\u7d61\u5148\uff1a 022-217-5660(\u62c5\u5f53\u8005\uff1a\u6280\u8853\u8077\u54e1\u30fb\u5343\u8449)<\/div>\n

\u9ad8\u901f\u30e9\u30de\u30f3\u30a4\u30e1\u30fc\u30b8\u30f3\u30b0\u30b7\u30b9\u30c6\u30e0<\/h2>\n

\u6a5f\u5668\u540d\uff1a\u5171\u7126\u70b9\u30e9\u30de\u30f3\u30de\u30a4\u30af\u30ed\u30b9\u30b3\u30fc\u30d7
\n\u88fd\u9020\u5143\uff1aRenishaw
\n\u578b\u756a\u3000\uff1ainVia Reflex\/Stream Line
\n\u7269\u8cea\u306e\u7a2e\u985e\u3084\u7d50\u6676\u306e\u72b6\u614b\u7b49\u3092\u8abf\u3079\u308b\u305f\u3081\u306b\u7528\u3044\u307e\u3059\u3002\u3053\u306e\u88c5\u7f6e\u3067\u306f1\u03bcm\u306e\u9ad8\u3044\u7a7a\u9593\u5206\u89e3\u80fd\u304c\u3042\u308a\u3001\u30e9\u30a4\u30f3\u30d5\u30a9\u30fc\u30ab\u30b9\u3084\u30de\u30c3\u30d4\u30f3\u30b0\u3092\u975e\u63a5\u89e6\u3001\u975e\u7834\u58ca\u3067\u884c\u3046\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002<\/p>\n

\"\"<\/a><\/p>\n

\u8a2d\u7f6e\u5834\u6240\uff1a\u5171\u540c\u7814\u7a76\u68df\u3000\u5b9f\u9a13\u5ba42
\n\u7ba1\u7406\u8005\uff1a \u67f4\u7530\u60a6\u90ce\u3000\u6559\u6388
\n\u9023\u7d61\u5148\uff1a 022-217-5213<\/div>\n","protected":false},"excerpt":{"rendered":"

\u6838\u78c1\u6c17\u5171\u9cf4\u88c5\u7f6e (\u6eb6\u6db2\u7528NMR 400\/500\/600MHz) \u6a5f\u5668\u540d\uff1a\u6838\u78c1\u6c17\u5171\u9cf4\u88c5\u7f6e NMR 400\/500\/600 MH…<\/p>\n","protected":false},"author":1,"featured_media":0,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"","meta":{"_locale":"ja","_original_post":"https:\/\/www2.tagen.tohoku.ac.jp\/lab\/caf\/?page_id=9","footnotes":""},"class_list":["post-9","page","type-page","status-publish","hentry","ja"],"_links":{"self":[{"href":"https:\/\/www2.tagen.tohoku.ac.jp\/lab\/caf\/wp-json\/wp\/v2\/pages\/9","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/www2.tagen.tohoku.ac.jp\/lab\/caf\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/www2.tagen.tohoku.ac.jp\/lab\/caf\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/www2.tagen.tohoku.ac.jp\/lab\/caf\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/www2.tagen.tohoku.ac.jp\/lab\/caf\/wp-json\/wp\/v2\/comments?post=9"}],"version-history":[{"count":21,"href":"https:\/\/www2.tagen.tohoku.ac.jp\/lab\/caf\/wp-json\/wp\/v2\/pages\/9\/revisions"}],"predecessor-version":[{"id":165,"href":"https:\/\/www2.tagen.tohoku.ac.jp\/lab\/caf\/wp-json\/wp\/v2\/pages\/9\/revisions\/165"}],"wp:attachment":[{"href":"https:\/\/www2.tagen.tohoku.ac.jp\/lab\/caf\/wp-json\/wp\/v2\/media?parent=9"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}